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Registro Completo |
Biblioteca(s): |
Embrapa Soja. |
Data corrente: |
15/08/2017 |
Data da última atualização: |
03/11/2017 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Autoria: |
AKAMATSU, H.; YAMANAKA, N.; SOARES, R. M.; IVANCOVICH, A. J. G.; LAVILLA, M. A.; BOGADO, A. N.; MOREL, G.; SCHOLZ, R.; YAMAOKA, Y.; KATO, M. |
Afiliação: |
JIRCAS; JIRCAS; RAFAEL MOREIRA SOARES, CNPSO; INTA - EEA PERGAMINO; NATIONAL UNIVERSITY OF THE NORTHWEST PROVINCE OF BUENOS AIRES; IPTA-CICM; IPTA - CICM; IPTA - CICM; UNIVERSITY OF TSUKUBA; JIRCAS. |
Título: |
Pathogenic variation of South American Phakopsora pachyrhizi populations isolated from soybeans from 2010 to 2015. |
Ano de publicação: |
2017 |
Fonte/Imprenta: |
JARQ: Japan Agricultural Research Quarterly, Tokyo, v. 51, n. 3, p. 221-232, 2017. |
ISSN: |
2185-8896 |
DOI: |
10.6090/jarq.51.221 |
Idioma: |
Português |
Thesagro: |
Doença de planta; Ferrugem; Fungo; Phakopsora pachyrhizi; Soja. |
Thesaurus Nal: |
Microbial growth; Plant diseases and disorders; Soybean rust. |
Categoria do assunto: |
F Plantas e Produtos de Origem Vegetal |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/162702/1/Akamatsu-et-al-2017-Pathogenic-variation-rust-51-03-221-232.pdf
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Marc: |
LEADER 01002naa a2200337 a 4500 001 2074022 005 2017-11-03 008 2017 bl uuuu u00u1 u #d 022 $a2185-8896 024 7 $a10.6090/jarq.51.221$2DOI 100 1 $aAKAMATSU, H. 245 $aPathogenic variation of South American Phakopsora pachyrhizi populations isolated from soybeans from 2010 to 2015.$h[electronic resource] 260 $c2017 650 $aMicrobial growth 650 $aPlant diseases and disorders 650 $aSoybean rust 650 $aDoença de planta 650 $aFerrugem 650 $aFungo 650 $aPhakopsora pachyrhizi 650 $aSoja 700 1 $aYAMANAKA, N. 700 1 $aSOARES, R. M. 700 1 $aIVANCOVICH, A. J. G. 700 1 $aLAVILLA, M. A. 700 1 $aBOGADO, A. N. 700 1 $aMOREL, G. 700 1 $aSCHOLZ, R. 700 1 $aYAMAOKA, Y. 700 1 $aKATO, M. 773 $tJARQ: Japan Agricultural Research Quarterly, Tokyo$gv. 51, n. 3, p. 221-232, 2017.
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Embrapa Soja (CNPSO) |
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Biblioteca(s): |
Embrapa Uva e Vinho. |
Data corrente: |
07/02/2017 |
Data da última atualização: |
06/05/2019 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 1 |
Autoria: |
SILVA, L. F. da; GUERRA, C. C.; KLEIN, D.; BERGOLD, A. M. |
Afiliação: |
LETICIA FLORES DA SILVA, CNPUV; CELITO CRIVELLARO GUERRA, CNPUV; Diandra Klein, Faculdade de Farmácia, Universidade de Caxias do Sul; Ana Maria Bergold, Laboratório de Química Farmacêutica, Universidade Federal do Rio Grande do Sul. |
Título: |
Solid cation exchange phase to remove interfering anthocyanins in the analysis of other bioactive phenols in red wine. |
Ano de publicação: |
2017 |
Fonte/Imprenta: |
Food Chemistryl, v. 227, p. 158-165, 2017. |
DOI: |
http://dx.doi.org/10.1016/j.foodchem.2017.01.087 |
Idioma: |
Inglês |
Conteúdo: |
Bioactive phenols (BPs) are often targets in red wine analysis. However, other compounds interfere in the liquid chromatography methods used for this analysis. Here, purification procedures were tested to eliminate anthocyanin interference during the determination of 19 red-wine BPs. Liquid chromatography, coupled to a diode array detector (HPLC-DAD) and a mass spectrometer (UPLC-MS), was used to compare the direct injection of the samples with solid-phase extractions: reversed-phase (C18) and strong cation-exchange (SCX). The HPLC-DAD method revealed that, out of 13 BPs, only six are selectively analyzed with or without C18 treatment, whereas SCX enabled the detection of all BPs. The recovery with SCX was above 86.6% for eight BPs. Moreover, UPLC-MS demonstrated the potential of SCX sample preparation for the determination of 19 BPs. The developed procedure may be extended to the analysis of other red wine molecules or to other analytical methods where anthocyanins may interfere. Chemical compounds studied in this article trans-Resveratrol (PubChemCID: 445154); trans-?-Viniferin (PubChemCID: 5315233); Quercetin (PubChemCID: 5280343); Myricetin (PubChemCID: 5281672); Kaempferol (PubChemCID: 5280863); trans-Cinnamic acid (PubChemCID: 444539); trans-Piceid (PubChemCID: 5281718); Taxifolin (PubChemCID: 439533) Keywords Bioactive phenols; Red wine; Liquid chromatography; Mass spectrometry; Diode array detector; Sample purification |
Palavras-Chave: |
Bioactive phenols; Diode array detector; Mass spectometry; Red wine; Sample purification. |
Thesaurus NAL: |
Liquid Chromatography. |
Categoria do assunto: |
-- |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/item/154893/1/Published-version-2017.pdf
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Marc: |
LEADER 02219naa a2200241 a 4500 001 2062946 005 2019-05-06 008 2017 bl uuuu u00u1 u #d 024 7 $ahttp://dx.doi.org/10.1016/j.foodchem.2017.01.087$2DOI 100 1 $aSILVA, L. F. da 245 $aSolid cation exchange phase to remove interfering anthocyanins in the analysis of other bioactive phenols in red wine.$h[electronic resource] 260 $c2017 520 $aBioactive phenols (BPs) are often targets in red wine analysis. However, other compounds interfere in the liquid chromatography methods used for this analysis. Here, purification procedures were tested to eliminate anthocyanin interference during the determination of 19 red-wine BPs. Liquid chromatography, coupled to a diode array detector (HPLC-DAD) and a mass spectrometer (UPLC-MS), was used to compare the direct injection of the samples with solid-phase extractions: reversed-phase (C18) and strong cation-exchange (SCX). The HPLC-DAD method revealed that, out of 13 BPs, only six are selectively analyzed with or without C18 treatment, whereas SCX enabled the detection of all BPs. The recovery with SCX was above 86.6% for eight BPs. Moreover, UPLC-MS demonstrated the potential of SCX sample preparation for the determination of 19 BPs. The developed procedure may be extended to the analysis of other red wine molecules or to other analytical methods where anthocyanins may interfere. Chemical compounds studied in this article trans-Resveratrol (PubChemCID: 445154); trans-?-Viniferin (PubChemCID: 5315233); Quercetin (PubChemCID: 5280343); Myricetin (PubChemCID: 5281672); Kaempferol (PubChemCID: 5280863); trans-Cinnamic acid (PubChemCID: 444539); trans-Piceid (PubChemCID: 5281718); Taxifolin (PubChemCID: 439533) Keywords Bioactive phenols; Red wine; Liquid chromatography; Mass spectrometry; Diode array detector; Sample purification 650 $aLiquid Chromatography 653 $aBioactive phenols 653 $aDiode array detector 653 $aMass spectometry 653 $aRed wine 653 $aSample purification 700 1 $aGUERRA, C. C. 700 1 $aKLEIN, D. 700 1 $aBERGOLD, A. M. 773 $tFood Chemistryl$gv. 227, p. 158-165, 2017.
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